The van Genuchten PURE LabPollutant Upcycling and Remediation Engineering
Our approach

Synchrotron methods and chemical experiments

We use complementary measurements to understand what contaminants are bound to, how they react, and what recovery processes produce.

Researcher adjusting equipment at an X-ray experimental station
Preparing an X-ray measurement. Photo: Dawn Harmer / SLAC National Accelerator Laboratory.

Synchrotron characterization

X-ray absorption spectroscopy probes oxidation state and local bonding environments. Spatially resolved spectroscopy and imaging reveal how elements are distributed within heterogeneous samples.

From spectra to process understanding

We use these observations alongside chemical experiments to test explanations for contaminant removal, extraction, and transformation.

Chemical experiments

Extraction, separation, precipitation, and redox transformations link environmental materials with recovery pathways.

Structure & speciation

Synchrotron spectroscopy, imaging, and structural characterization connect composition with reactivity.

Environmental assessment

We examine the implications of treatment and residual management, including life-cycle perspectives.

See the methods in our publications →
Speciation in heterogeneous samples

Where is phosphorus, and what is it bound to?

X-ray fluorescence maps locate elements within the sample. Micro-XANES measurements at selected positions then provide information about phosphorus speciation. The overview below connects sample preparation, beamline measurements, and the resulting maps.

SSRL overview of sample preparation, elemental mapping, and micro-XANES for phosphorus speciation
Sample preparation, elemental maps, and micro-XANES measurements for phosphorus speciation at SSRL. Click to enlarge.
A shared research framework

Characterization, extraction, and valorization

A conceptual framework connects the chemical forms of elements in sludge and fly ash with extraction and potential product formation. This schematic describes research pathways rather than a claim that every route has been demonstrated.

Conceptual molecular-scale pathways for characterization, extraction, and valorization of sludge and fly ash
Conceptual recovery pathways for arsenic, antimony, and phosphorus. Click to enlarge.